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Atsushi Waseda, Kenichi Fujii
DENSITY MEASUREMENT OF A THIN-FILM BY THE PRESSURE-OF-FLOTATION METHOD

A method for density and thickness measurements of a thin-film is described by the pressure-offlotation method (PFM). The density and thickness of a silicon thermal oxide layer on silicon crystal are determined by measuring the density and mass differences for the sample with and without the thin-film. Details on the density and thickness measurement and the results of the measurements are presented.

Barry Pratt, Andy Robinson
A COMPARISON BETWEEN SUPPORTED AND UNSUPPORTED BEAMS FOR USE IN STATIC TORQUE CALIBRATIONS

In industry, calibration beams are frequently coupled directly to the measurement transducer. This paper aims to quantify the effect of using such a method in contrast to the bearing supported case for a range of commercially available transducers.

Yon-Kyu Park, Rolf Kumme, Dae-Im Kang
DYNAMIC EVALUATION OF COLUMN TYPE MULTI-COMPONENT FORCE TRANSDUCERS

This paper describes the dynamic characteristics of column type 6-component force-moment sensors with force components Fx, Fy, Fz and moment components Mx, My, Mz. We have evaluated the dynamic characteristics of the force-moment sensors by using a shaker system and a multi-channel dynamic analyzer system. It reveals that the sensitivity decreases as the frequency increases except for the Fz component and that the sensor shows almost 90° symmetry due to its geometry.

Ricardo Luís da Rocha Carmona, Sílvio Fazolli, Milton Pereira
MENIR – A CONTRIBUTION FOR FINAL UNCERTANTY EVALUATION OF ROCKETS MASS MEASUREMENTS

The weight is a very significant property for several rocket projects’ calculations. The cost of satellite mass is very high and a reduction of 1% can save thousands of dollars. Then it’s necessary to know the most important uncertainty sources to obtain a reliable result. In this paper, a developed method is shown to find the smaller uncertainty of a rocket’s weight among several available weighing instrument parks.

Sheau-Shi Pan,Hui-Ching Lu, Chi-Sheng Chang
EVALUATING THE UNCERTAINTY FOR MAGNETIC SUSCEPTIBILITY USING THE DIRECTLY METHOD

The volume magnetic susceptometer was established in the CMS mass laboratory in 2003. The method is referred to the experimental method and procedure developed by Davis; while the distances between weighs and the magnetic sample were measured with the laser interferometer. We calculated the effect by the offset between the magnetic source and the weights; then we evaluated the uncertainty of the χ-value in samples directly.

Edi Kulderknup, Viktor Krutob, Jürgen Riim
UNCERTAINTY OF BRAKING PARAMETERS MEASUREMENTS BY VEHICLES TECHNICAL INSPECTION

Nowadays more widely is taken to use the road vehicles periodical inspection with aim to have knowledge of the technical level of item and to assure the safety. To have the assured right inspection results there shall be used various testing and measurement procedures. Among of the important are measurements of the parameters showing the road vehicles brakes correct operation. To give proper conformity estimation to the vehicles brakes operation shall be used uncertainty of measurement result. To give more confidence to the estimated uncertainty components suitable way is to carry out measurement comparisons of brakes parameters.

Naoki Kuramoto, Kenichi Fujii
ABSOLUTE VOLUME MEASRUMENET OF SILICON SPHERES AT NMIJ

The method and devices for absolute volume measurements of 1 kg silicon spheres are described. An interferometer equipped with a direct optical frequency tuning system is used to measure the sphere volume, in which the optical frequency of a diode laser can be tuned continuously over a frequency range of 19 GHz. Accurate frequency changes in the laser produced by this system are used to measure the sphere diameters by phase-shifting interferometry. A total of seventy diameters, which are distributed near-uniformly over the surface of the sphere, are measured in vacuum. The volume of the sphere is determined by fitting the diameters to a series of spherical harmonics. The mass of the sphere is compared with that of the national prototype of the kilogram through a secondary 1 kg standard. The relative combined standard uncertainty in the density determined by direct measurements of the mass and volume is presently estimated to be 7.3·10-8. Recent results on the volume determination for three 1 kg silicon spheres are shown.

Maria do Céu Ferreira, José Mendonça Dias
THE ROLE OF EXPERIMENTAL DESIGN IN THE HYDROMETER FIELD

The main purpose of this paper is to study the uncertainty budget of hydrometers calibration and the error of Cuckow’s method according the Signal-to-Noise Ratio Taguchi approach in order to analyse this two different kinds of methodology. The calibration of density hydrometers is influenced by some parameters; in order to research the influence of these factors in the measuring value, an experimental design with dynamic characteristics was applied. With this methodology, five control factors were considered, at two levels each and a L32 Orthogonal Array was defined. It was evaluated the influence of each parameter (factor) and the interaction between them according Cuckow’s method and Taguchi methodologies. The simultaneous analysis of the error and the sensitivity leads to a proper choice of significant control factors and respective best levels in order to reduce the variability of the measurement system.

Marisa Ferraz Figueira Pereira, Jorge Antonio da Paz Cruz, Walter Link, Luiz Carlos Cabral de Freitas Link, Antonio Carlos Marques Garcia
DEVELOPMENT AND MANUFACTURE OF CHARPY STANDARDS TEST SPECIMENS FOR XVIII IMEKO WORLD CONGRESS

The main purpose of this presentation is to show the development of standard test specimens to be used in indirect calibration of Pendulum-Type Impact Testing Machines, performed by the Mechanical Metrology Laboratory–LMM-IPT and the Force Laboratory – LAFORINMETRO. LMM-IPT is an accredited laboratory, in force, by RBC, the Brazilian Accreditation Net. INMETRO is the reference metrological institute in Brazil.

W. Holzapfel, M. Suske
PRECISE FORCE MEASUREMENTS BY PHOTO-ELASTIC LASER CRYSTALS IN THE TIME /FREQUENCY DOMAIN

Mechanical forces can be sensed over a very broad input range (10 nN up to 100 kN) with high resolution and linearity by applying the photo-elastic effect in small solid-state lasers (diode-pumped Nd:YAG crystals). The input force vector modulates the optical frequency of the laser crystal. In our experiments sinusoidal, pulse, and transient forces are generated by a PCT drive in a special dynamic test set up. By simple autodyne detection of the laser beam and concurrent signal processing of the electrical beat signal, we can measure sinusoidal forces from DC up to 100 kHz modulation frequency. Frequency counter measurement of pulse forces can be performed within few microseconds. By digital filtering, the final value of structure-induced transient forces can be predicted with high precision in milliseconds.

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